QV if there are any pics taken, I'd love to see them.
Seeing the PR with a huge grin on her face would make my da...wee..not sure how long but quite some time.
Another thing currently making me happy is getting the toolshed to myself all night. Hopefully now I can get to production of some violet phosphorus.
The preparation takes a long time, 24 hours at least, heating a sample of elemental phosphorus in molten lead, and then dissolving the lead away with acid to reveal the violet phosphorus within.
Going to try it with both red and white phosphorus and see if there is any difference, or if one succeeds and the other does not. Red P comes as a powder, and I've 2kg to play with so to speak, and the only time I've seen violet phosphorus on sale on ebay, it was going for about £20 PER GRAM. Not reactive much, unlike white phosphorus, and like red P, its not pyrophoric, and it is not known, unlike white phosphorus to be highly toxic. I want to try making some lead molds, filling them with white phosphorus by melt-casting, then topping it off with more molten lead.
First, I shall have to get out my alembic and begin purging it with argon, and leading the outlet into hot water, to melt the recovered white phosphorus. Got plenty to try with, in fact I might just try it on test-tube scale first and see if my hotplate alone will reach the transition point, or if I need to frabricate a metal distillation vessel.
First things first though, I'm finishing my can of beer, jar of pickled olives and jelly-babies (love the black and thee green ones...biting their little baby toes off, and pulling their heads off..yum)
And finishing my rollup.