Room for one more ? you two would be just the kind of company as would be good right now, the fiery and delightful miss K with the mood I'm in at my old man after he just poured some of a long-worked for and hard worked for multi-step synthesis that was going to finish to...celebrate..my b/day being too stupid to realize it was something of mine. Weeks of work to say nothing of the pre-study experimentation...almost the final fruition of my project after the time spent in purification. Kind of easy reaction but does requite a lot of cleaning of more or less each phase to reach the required standard. Down the bastard drains.I'll have to work it out by thorough cleaning of the adduct of one of the byproducts and calculate from the theoretical plus the weight of the byproducts. I think Hyke would keep me grounded, if that makes sense